Fraction Collection

Specifications

Ordering Information

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Documentation

Overview

Fraction Collection using Valves

Overview

Knauer rotary valves offer a low-cost flexible solution for fraction collection in preparative chromatography. Valves with six, twelve or sixteen ports are available in either stainless steel or peek versions. Positioning is controlled via a standard electric valve drive module which can be controlled either manually or using remote control.
 
Fraction Collection Software
Use of the Knauer Fraction Collection software option fully automates the application and allows also solventor peak recycling if required.
 
Inert Collection Possibilities
Using these valves it is possible to design systems where the process occurs with complete isolation of the sample or product. Fractions are collected directly into standard laboratory bottles which can be fitted with quick-connect adapters to allow rapid and safe exchange of bottles as required.

Smartline 7/1 Distribution Valve
 

Standard Fraction Collectors

Smartline Fraction Collector 3050
 
The ultra fast drive enables position changes in very short times, allowing collection of very narrow peaks, for instance in UHPLC.
The Smartline Fraction Collector 3050 is available in two versions: an analytical version for flow rates up to 5 ml/min with cover and optional sample cooling or a semi-präparative version for flow rates up to 50 ml/min. The fraction collector can collect up to 384 fractions in well plates or up to 192 fractions in standard autosampler vials.
Due to the identical rack design the racks can be transferred directly to autosamplers such as the Smartline Autosampler 3950. Special racks for different test tubes, beakers or flasks up to 250 ml also can be used.
The fraction collector can be controlled with ChromGate® software, with or without the FRC option, or ClarityChrom® Prep via LAN or RS232.
Sensitive samples can be protected against warming using the cooling option. A solvent and peak recycling option with two additional valves is available for saving solvents and costs.

Smartline 3050 Fraction Collector Module
 
Foxy® R1 Fraction Collector

Fraction Collector Foxy® R1
 
The Foxy® R1 is the improved successor of the well-known Foxy® Jr. and can be used for a variety of applications. The Foxy® R1 accomodates the same rack types as its predecessor, but provides faster operation, more control options (RS-232 and Ethernet) and features an integrated diverter valve as a standard. When connected to a detector, the Foxy® R1 offers slope detection, level sensing, and a combination of these methods. The applicable rack types range from 96-well microplates, to test tube racks, to funnel racks for virtually unlimited collection volumes. The Foxy® R1 is biocompatible and can be used in cold room environments
Foxy® R1 can be fully controlled using either the ChromGate® software together with the Fraction Collector Control Option or with our Geminyx Software.

 
 

Specifications

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Smartline 6 / 12 / 16 Port Distributor Valves

Display

LED

Switching time

<150 ms

External control

RS-232 connector, shorting contacts for position 1 and next position or binary code

Dimensions (mm)

85 x 100 x 150 (W x H x D)

Weight

0.8 kg

Smartline Fraction Collector 3050

 

Analytical Version

Semi-preparative Version

Sample Vials

4 x 96 deep well plates, 4 racks with 48 vials 1.5 ml, 4 racks with 12 vials 5 or 10 ml

4 racks with 48 test tubes 12 mm OD, 4 racks with 24 test tubes 16 mm OD, 4 racks with 24 test tubes 18 mm OD, 4 racks with 12 test tubes 25 mm OD, 4 racks for 2 beakers or bottles max. 250 ml

Flowrate

0.1 – 5 ml/min.

1 – 50 ml/min

Maximum pressure

3 bar

3 bar

Switching time

100 ms

100 ms

Delay volume (approx.)

40 µl

300 µl

Optional valves

Solvent and peak recycling valves

Solvent and peak recycling valves

Foxy® R1

Sample Vials

12 mm diameter tubes (144/rack), 13 mm diameter tubes (144/rack), 16 mm diameter tubes (100/rack), 18 mm diameter tubes (72/rack), 25 mm diameter tubes (36/rack), 1.5 ml microcentrifuge tubes (60/rack), 50 ml centrifuge tubes (36/rack), 28 mm diameter scintillation vials (36/rack), 96-well microplates (up to 2 plates total), MiniVials (72/rack), 480 ml bottles, Funnel racks for fractions larger than 480 ml

Collection control

Time, drop number and volume control, if a suitable detector is connected peak detection according to time, signal level, and signal slope is possible.

Flowrate

max. 25 ml/min.

Switching time

200 to 450 ms

Temperature range

0°C - 40°C

External control

RS-232 with ChromGate or ClarityChrom software, Ethernet

All specifications may be subject to change for technical reasons.

 

 
Ordering Information
 

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A55030

Smartline Electrical Valve Drive 7-Port/1-Channel switching valve, stainless steel, 1/16" connections with external power supply included

A55040

Smartline Electrical Valve Drive 7-Port/1-Channel switching valve, stainless steel, 1/8" connections with external power supply included

A55110

Smartline Electrical Valve Drive 13-Port/1-Channel switching valve, stainless steel, 1/8" connections with external power supply included

A55211

Smartline Electrical Valve Drive 17-Port/1-Channel switching valve, stainless steel, 1/16", maximum 100 bar, and external power supply included

A5371

Smartline Fraction Collector 3050, analytical version

A5372

Smartline Fraction Collector 3050, semi-preparative version

A59100

Fraction Collector Foxy® R1 with integrated diverter valve, including rack for 13 mm vials, other racks are also available.

 

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